Structural and mechanical properties of stainless steel formed under conditions of layer-by-layer fusion of a wire by an electron beam

OBRABOTKAMETALLOV Vol. 23 No. 4 2021 122 MATERIAL SCIENCE Structural and mechanical properties of stainless steel formed under conditions of layer-by-layer fusion of a wire by an electron beam Vasiliy Fedorov 1, a, * , Aleksandr Rygin 2, b , Vasiliy Klimenov 1, c , Nikita Martyushev 1, d , Anatolii Klopotov 2, 3, e , Irina Strelkova 1, f , Sergey Matrenin 1, g , Andrey Batranin 1, h , Valentina Deryusheva 1, i 1 National Research Tomsk Polytechnic University, 30 Lenin ave., Tomsk, 634050, Russian Federation 2 Tomsk State University of Architecture and Building, 2 Solyanaya Sq., Tomsk, 634003, Russian Federation 3 National Research Tomsk State University, 36 Lenin ave., Tomsk, 634050, Russian Federation a https://orcid.org/0000-0002-5164-5875, fedorov@tpu.ru, b https://orcid.org/0000-0001-5664-8234, alexandr.rygin@gmail.com, c https://orcid.org/0000-0001-7583-0170, klimenov@tpu.ru , d https://orcid.org/0000-0003-0620-9561, martjushev@tpu.ru, e https://orcid.org/0000-0002-3690-0436, klopotovaa@tsuab.ru , f https://orcid.org/0000-0002-2222-2865, strelkova@tpu.ru , g https://orcid.org/0000-0002-2188-8120, msv@tpu.ru , h https://orcid.org/0000-0001-9678-2905, batranin@tpu.ru , i https://orcid.org/0000-0002-2116-3891 , vderusheva@tpu.ru Obrabotka metallov (tekhnologiya, oborudovanie, instrumenty) = Metal Working and Material Science. 2021 vol. 23 no. 4 pp. 111–124 ISSN: 1994-6309 (print) / 2541-819X (online) DOI: 10.17212/1994-6309-2021-23.4-111-124 Obrabotka metallov - Metal Working and Material Science Journal homepage: http://journals.nstu.ru/obrabotka_metallov ARTICLE INFO Article history : Received: 02 September 2021 Revised: 16 September 2021 Accepted: 23 September 2021 Available online: 15 December 2021 Keywords : Additive technologies Electron beam surfacing Stainless steel Coarse austenitic steel Funding This research was supported by TPU development program. Acknowledgements Research were conducted at core facil- ity “Structure, mechanical and physi- cal properties of materials”. ABSTRACT Introduction. As of today, additive technologies are among the most promising methods to manufacture vari- ous parts. They allow producing parts of complex shapes and provide their quality structure. The quality of the structure formed depends on numerous parameters: equipment type, its operation mode, materials, shielding me- dium, etc. Large international companies producing 3D-printers provide technological guidelines for working on it. Such guidelines include the information on the manufacturers of raw materials (printing powders), products their equipment can work with and the operation modes that should be used with such powders. These parameters should be investigated to use it on the domestic equipment developed within the framework of research programs and import substitution programs. The researchers and developers of 3D-printing equipment frequently run into a problem of using currently available raw materials for obtaining parts possessing minimal porosity, uniform structure and mechanical properties similar to that of at least cast blanks. One of the widely used materials for 3D-printing is stainless steel. It has high corrosion resistance, which reduces the requirements to the medium in which 3D printing is carried out. Manufactured stainless steel products have a good combination of strength and plastic characteristics. The aim of the study is to obtain stainless steel specimens possessing minimal number of micro- and macro-defects and uniform structure by the method of wire arc additive manufacturing using an electron-beam setup developed at Tomsk Polytechnic University. The methods to study the AISI 308LSi stainless steel 3D-printed specimens are as follows: XRD analysis, tomography, chemical analysis, metallographic analysis, microhardness testing. Results and discussion. It is established that the AISI 308LSi stainless steel specimens manufactured using the electron-beam 3D- printing setup contain no macro-defects in the bulk of the specimens. There are small microdefects represented by residual gas pores with the dimensions of no more than 5.2 μ m. The microstructure of the specimens is formed close to that of coarse-grained cast austenite steels and consists of columnar grains of the γ -Fe austenite matrix and high- temperature ferrite. The interfaces between the wire layers are not pronounced; however, there are small differences in phase composition. Based on the analysis of the results obtained, it is established that the use of electron-beam 3D-printing for the manufacture of parts from AISI 308LSi steel gives a structure similar to cast austenitic steels. Macro-defects do not appear, and the number of gas pores is small. For citation: Fedorov V.V., Rygin A.V., Klimenov V.A., Martyushev N.V., Klopotov A.A., Strelkova I.L., Matrenin S.V., Batranin A.V., Deryusheva V.N. Structural and mechanical properties of stainless steel formed under conditions of layer-by-layer fusion of a wire by an electron beam. Obrabotka metallov (tekhnologiya, oborudovanie, instrumenty) = Metal Working and Material Science , 2021, vol. 23, no. 4, pp. 111–124. DOI: 10.17212/1994-6309-2021-23.4-111-124. (In Russian). ______ * Corresponding author Fedorov Vasiliy Viktorovich , Laboratory manager National Research Tomsk Polytechnic University, 30 Lenin ave., 634050, Tomsk, Russian Federation Tel.: 8 (3822) 606006, e-mail: fedorov@tpu.ru