Proceedings of the RHSAS

PROCEEDINGS OF THE RUSSIAN HIGHER SCHOOL
ACADEMY OF SCIENCES

Print ISSN: 1727-2769    Online ISSN: 2658-3747
English | Русский

Recent issue
№2(67) April - June 2025

Modification of diffusion boron and aluminum containing layers by electron beam processing

Issue No 1 (62) January - March 2024
Authors:

Ulakhanov Nikolay Sergeevich,
Moskvin Pavel Vladimirovich,
Mishigdorzhiyn Undrakh Lkhagvasurenovich,
Semenov Alexander Petrovich,
Koval Nikolai Nikolaevich,
Vorobyov Maxim Sergeevich
DOI: http://dx.doi.org/10.17212/1727-2769-2024-1-62-75
Abstract

The article presents testing results of electron beam processing (EBP) modes applied on the diffusion layers based on boron and aluminum produced on the surface of steel 20. An ion current feedback loop in the accelerating gap in a modernized plasma electron source allows increasing the beam generation control and the electrical strength of the accelerating gap. This ensures sample surface processing at a specified temperature. In order to ensure the EBP process stability, it is proposed to preheat the surface to a temperature range of 400-700? by pulses with a controlled current. Further modification of the diffusion layers is conducted on the surface at a temperature of around 1900?. Ensuring this temperature range demands the discharge current within the range of 20 - 150A during a single pulse with a duration of 950 μs. The total number of pulses is three and the interval between them is 3 seconds. These processing modes lead to a structural transformation of the diffusion layer to a depth of more than 150 μm and to a significant microhardness increase. The approved EBP modes can be recommended as a promising alternate approach of the combined modification technologies of diffusion layers based on boron and aluminum.


Keywords: thermal-chemical treatment, boroaluminizing, pulsed electron beam processing, microhardness, electron source, plasma cathode, electron beam power adjustment

References
  1. Devyatkov V.N., Koval N.N., Schanin P.M., Grigoryev V.P., Koval T.V. Generation and propagation of high-current low-energy electron beams. Laser and Particle Beams, 2003, vol. 21 (2), pp. 243–248. DOI: 10.1017/S026303460321212X.
  2. Grigoriev S.V., Devyatkov V.N., Mikov A.V., Moskvin P.V., Teresov A.D. Elektronno-puchkovaya ustanovka «SOLO-M» dlya modifikatsii poverkhnosti metallicheskikh i metallokeramicheskikh materialov [E-beam installation "SOLO-M" for surface modification metallic and cermet materials]. Izvestiya vysshikh uchebnykh zavedenii. Fizika = Russian Physics Journal, 2014, vol. 57, no. 11-3, pp. 58–62.
  3. Devyatkov V.N., Ivanov Yu.F., Krysina O.V., Koval N.N., Petrikova E.A., Shugurov V.V. Equipment and processes of vacuum electron-ion plasma surface engineering. Vacuum, 2017, vol. 143, pp. 464–472. DOI: 10.1016/j.vacuum.2017.04.016.
  4. Shin V.I., Vorob'ev M.S., Moskvin P.V., Devyatkov V.N., Yakovlev V.V., Koval' N.N., Torba M.S., Kartavtsov R.A., Vorob'ev S.A. Shirotnaya i amplitudnaya modulyatsiya toka puchka dlya upravleniya ego moshchnost'yu v techenie impul'sa submillisekundnoi dlitel'nosti [Latitude and amplitude modulation of the beam current for controlling its power during a submillisecond pulse]. Izvestiya vysshikh uchebnykh zavedenii. Fizika = Russian Physics Journal, 2022, vol. 65, no. 11, pp. 176–184. DOI: 10.17223/00213411/65/11/176.
  5. Gromov V.E., Ivanov Yu.F., eds. Struktura, fazovyi sostav i svoistva titana posle kompleksnykh uprochnyayushchikh tekhnologii [Structure, phase composition and properties of titanium after complex hardening technologies]. Novokuznetsk, SibSIU Publ., 2015. 306 p. ISBN 978-5-7806-0428-0.
  6. Ionina A.V., Budovskikh E.A., Konovalov S.V., Ivanov Y.F., Panchenko I.A., Gromov V.E. Modifikatsiya poverkhnosti tekhnicheski chistogo titana VT1-0 posle razlichnykh vidov obrabotki [Modification of the surface of technically pure titanium VT1-0 after various types of processing]. Izvestiya Yugo-Zapadnogo gosudarstvennogo universiteta. Seriya: Tekhnika i tekhnologii = Proceedings of the Southwest State University. Series: Engineering and Technologies, 2023, vol. 13 (1), pp. 21–31. DOI: 10.21869/2223-1528-2023-13-1-21-31.
  7. Konovalov S.V., Chen X., Gromov V.E., Komissarova I.A., Gleser A.M., Ivanov Y.F. Vliyanie elektronno-puchkovoi obrabotki na strukturu tekhnicheski chistogo titana, podvergnutogo ustalostnomu razrusheniyu [Effect of electron-beam treatment on the structure of commercial-purity titanium subjected to fatigue failure]. Deformatsiya i razrushenie materialov = Russian Metallurgy (Metally), 2019, no. 9, pp. 42–48. DOI: 10.31044/1814-4632-2019-9-42-48. (In Russian).
  8. Komissarova I.A., Konovalov S.V., Kosinov D.A., Feoktistov A.V., Ivanov Y.F., Gro­mov V.E. Formirovanie i evolyutsiya struktury i fazovogo sostava titana VT1-0 pri elektronno-puchkovoi obrabotke, tokovom impul'snom vozdeistvii i mnogotsiklovoi ustalosti [Formation and evolution of the structure and phase composition of titanium VT1-0 during electron beam processing, current pulse exposure and high-cycle fatigue]. Antologiya prochnosti i plastichnosti metallov i splavov pri vneshnikh energeticheskikh vozdeistviyakh [Anthology of strength and ductility of metals and alloys under external energy influences]. Novokuznetsk, SibSIU Publ., 2018, pp. 62–81.
  9. Koval N.N., Gromov V.E., eds. Struktura i svoistva tverdykh tel, podvergnutykh vysokointensivnomu vozdeistviyu (k 65-letiyu professora Yu.F. Ivanova) [Structure and properties of so­lids subjected to highly intense impact (to the 65th anniversary of Professor Yu.F. Ivanov)]. Novokuznetsk, Polygraphist Publ., 2020. 337 p. ISBN 978-5-91797-285-5.
  10. Ivanov Y.F., Bessonov D.A., Vorob'ev S.V., Gromov V.E., Konovalov S.V., Koval N.N. Ustalostnaya dolgovechnost' stali martensitnogo klassa, modifitsirovannoi vysokointensivnymi elektronnymi puchkami [Fatigue durability of martensitic steel modified with high-intensity electron beams]. Novokuznetsk, Inter-Kuzbass Publ., 2011. 259 p. ISBN 978-5-905647-01-7.
  11. Gromov V.E., Ivanov Y.F., Vorob'ev S.V., Gorbunov S.V., Bessonov D.A., Sizov V.V., Konovalov S.V. Ustalost' stalei, modifitsirovannykh vysokointensivnymi elektronnymi puchkami [Fatigue of steels modified with high-intensity electron beams]. / V. E. Gromov, Yu. F. Ivanov, S. V. Vorobyov [etc.]. Novokuznetsk, Inter-Kuzbass Publ., 2012. 403 p. ISBN 978-5-905647-02-4.
  12. Volkov K.V., Gromov V.E., Ivanov Y.F., Grishunin V.A. Povyshenie ustalostnoi vynoslivosti rel'sovoi stali elektronno-puchkovoi obrabotkoi [Increasing the fatigue endurance of rail steel by electron beam processing]. Novokuznetsk, Inter-Kuzbass Publ., 2013. 225 p. ISBN 978-5-905647-06-2.
  13. Gromov V.E., Ivanov Y.F., Borobiev S.V., Konovalov S.V. Fatigue of steels modified by high intensity electron beams. Cambridge, Cambridge International Science Publ., 2015. 272 p. ISBN 978-1-907343-53-7.
  14. Ulahanov N.S., Mishigdorjiyn U.L., Tihonov A.G., Shustov A.I., Pyatyih A.S. Modifikatsiya poverkhnostnogo sloya shtampovykh stalei sozdaniem B-Al-sloev khimiko-termicheskoi obrabotkoi [Surface modification of die steels with B–Al-layers by thermal-chemical treatment]. Uprochnyayushchie tekhnologii i pokrytiya = Strengthening technologies and coatings, 2021, vol. 17, no. 12 (204), pp. 557–564. DOI: 10.36652/1813-1336-2021-17-12-557-564.
  15. Koval N.N., Devyatkov V.N., Vorobyev M.S. Electron sources with plasma grid emitters: progress and prospects. Russian Physics Journal, 2021, vol. 63 (10), pp. 1651–1660. DOI: 10.1007/s11182-021-02219-3.
  16. Koval N.N., Grigoryev S.V., Devyatkov V.N., Teresov A.D., Schanin P.M. Effect of intensified emission during the generation of a submillisecond low-energy electron beam in a plasma-cathode diode. IEEE Transactions on Plasma Science, 2009, vol. 37 (10), pp. 1890–1896. DOI: 10.1109/TPS.2009.2023412.
  17. Kompleks unikal'nykh elektrofizicheskikh ustanovok dlya effektivnoi elektronno-ionno-plazmennoi modifikatsii poverkhnosti materialov i izdelii «UNIKUUM» [Complex of unique electrophysical installations for effective electron-ion-plasma modification of the surface of materials and products “UNICUUM”]. NTIRF Portal. (In Russian). Available at: https://ckp-rf.ru/catalog/usu/434216/ (accessed 06.03.2024).
  18. Vorobyov M.S., Moskvin P.V., Shin V.I., Koval T.V., Devyatkov V.N., Doroshkevich S.Y., Koval N.N., Torba M.S., Ashurova K.T. Negative current feedback in the accelerating gap in electron sources with a plasma cathode. Technical Physics, 2022, vol. 67 (6), pp. 747–752. DOI: 10.21883/TP.2022.06.54422.14-22.
  19. Vorobev M.S., Koval T.V., Koval N.N., et al. Sposob generatsii elektronnogo puchka dlya elektronno-puchkovoi obrabotki poverkhnosti metallicheskikh materialov [Electron beam generation method for electron beam treatment of metal materials surface]. Patent RF, no. 2746265 C1, 2021.
  20. Mishigdorzhiyn U., Chen Y., Ulakhanov N., Liang H. Microstructure and wear behavior of tungsten hot-work steel after boriding and boroaluminizing. Lubricants, 2020, vol. 8 (3). DOI: 10.3390/lubricants8030026.
  21. Mishigdorzhiyn U., Sizov I. The influence of boroaluminizing temperature on microstructure and wear resistance in low-carbon steels. Materials Performance and Characterization, 2018, vol. 7 (3), pp. 252–265. DOI: 10.1520/MPC20170074.
For citation:

Ulakhanov N.S., Moskvin P.V., Mishigdorzhiyn U.L., Semenov A.P., Koval N.N., Vorobyov M.S. Modifikat­siya diffuzionnykh bor- i alyuminii soderzhashchikh sloev elektron-no-puchkovoi obrabotkoi [Modification of diffusion boron and aluminum containing layers by electron beam processing]. Doklady Akademii nauk vysshei shkoly Rossiiskoi Federatsii = Proceedings of the Russian higher school Academy of sciences, 2024, no. 1 (62), pp. 62–75. DOI: 10.17212/1727-2769-2024-1-62-75.

Views: 433